11–13 Oct 2017
Hungarian Academy of Sciences
Europe/Budapest timezone

Non destructive determination of the manufacturing methods of ancient Indian blades and modern replicas through advanced applications of neutron tomography and neutron diffraction

11 Oct 2017, 16:40
20m
Hungarian Academy of Sciences

Hungarian Academy of Sciences

1051 Budapest, Széchenyi István tér 9.
Oral presentation Multi-technique approach and complementary techniques Multi-technique approach and complementary methods 1.

Speaker

Dr Francesco Grazzi (Consiglio Nazionale Ricerche)

Description

The analysis of the micro-structural features of ancient Indian blades has been carried out by neutron tomography and neutron diffraction. The results provide a clear identification of the different types of steel used to produce such weapons. Among them, only a small proportion of the large number of swords produced in India is made of hypereutectoid textured steel, namely wootz steel also known as “Damascus steel”. The others present characteristics very similar to the European swords produced in the same period including composite low and high carbon steel assembled together and the application of thermal treatments. The ancient swords and daggers, provided by the Wallace Collection in London and the Bernisches Historisches Museum in Bern, as well as the modern replicas made by a professional swordsmith, were analyzed using neutron tomography both in white beam and energy selective configurations and neutron diffraction to get quantitative phase analysis and pole figure reconstruction of the texture in cementite phase. The results permitted to determine the spatial distribution of the iron and steel components inside the swords and the size and orientation of the microstructure of the ferrite and cementite grains in the wootz steel. These results are an important starting point to lead to the comprehension of the metal preparation and the forging procedure to produce swords made of wootz steel. This kind of results is a further proof of the validity of the use of neutron techniques for non destructive and quantitative authentication and characterization of ancient metal artifacts.

Primary authors

Dr Alan Williams (The Wallace Collection, London, UK) Dr Burkhard Schillinger (Heinz Maier-Leibnitz Zentrum (FRM II)) Dr David Edge (The Wallace Collection, London, UK) Dr Francesco Grazzi (Consiglio Nazionale Ricerche)

Co-authors

Dr Anders Kaestner (Paul Scherrer Institut, Neutron Imaging and Activation Group, Villigen, Switzerland) Dr Antonella Scherillo (Science and Technology Facility Council, ISIS neutron source, Didcot, UK) Mr Davide Coco (Università di Roma “La Sapienza”, Roma, Italy) Dr Filomena Salvemini (Australian Nuclear Science and Technology Organisation, Bragg Institute, Lucas Heights, Australia) Mr Francesco Cantini (Università di Firenze, Firenze, Italy) Dr Weimin M. Gan (German Engineering Materials Science Centre at MLZ, Helmholtz-Zentrum Geesthacht, Garching, Germany)

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